HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11817172, compound → HCID 11287703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11817172 | HCID 11817172 | — |
| Solvent | Manganese dioxide | HCID 14801 | — |
| Solvent | dichloromethane N,N-dimethylformamide | HCID 22350042 | — |
| Product | HCID 11287703 | HCID 11287703 | — |
Reaction Steps
2-Formyl-7-methoxyimidazo[2,1-b]-benzthiazole was prepared according to the procedure outlined in Example 1, (Step 3). Starting from 7-methoxy imidazo[2,1-b]-benzthiazole-2-methanol (4.0 g 17 mmol) in methylene chloride/DMF(300 mL: 50 mL) and active MnO2 (12 g, excess), 822 mg (21% Yield) of the aldehyde derivative was isolated as brown solid. (M+H) 233.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018997B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-7b12780b0923413c94c4e98fc3d67851 |
| Source note | uspto-grants-2006_03 |