HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-methylbenzothiazole → HCID 394241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-methylbenzothiazole | HCID 15132 | — |
| Reactant | Ethyl bromopyruvate | HCID 66144 | — |
| Product | HCID 394241 | HCID 394241 | 47.3% |
Reaction Steps
Ethyl 5-methylimidazo[2,1-b]-benzthiazole-2-carboxylate was prepared according to the procedure as outlined in Example 1, (Step 1). Starting from 4-methly-2-amino benzothiazole (8.0 g, 48.7 m.mol) and ethyl bromopyruvate (14.0 g, 71.7 mmol), 6.0 g (45% Yield) of ethyl 5-methylimidazo[2,1-b]-benzthiazole-2-carboxylate was isolated as a brown solid. (M+H) 261.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018997B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-c2380077366340c79d38c71cb2e7c280 |
| Source note | uspto-grants-2006_03 |