HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 394241, compound → 5-Methylimidazo[2,1-b]benzothiazole-2-methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 394241 | HCID 394241 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 5-Methylimidazo[2,1-b]benzothiazole-2-methanol | HCID 11816822 | 69% |
Reaction Steps
5-methyl imidazo[2,1-b]-benzthiazole-2-methanol was prepared according to the procedure outlined in Example 1, (Step 2). Starting from ethyl 5-methylimidazo[2,1-b]-benzthiazole-2-carboxylate (5.2 g, 20 mmol) and LiAlH4 solution (22 ml, 0.5 M solution in THF), 3 g (69% yield) of the alcohol derivative was isolated as a brown solid. (M+H) 219.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018997B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-8e386c6f405a4141872e9b96093688e7 |
| Source note | uspto-grants-2006_03 |