HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(1H-pyrrol-1-yl)aniline → (2S,4EZ)-4-(tert-butoxyimino)-N-[2-(1H-pyrrol 1-yl)phenyl]-2-pyrrolidinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(1H-pyrrol-1-yl)aniline | HCID 80123 | — |
| Reactant | (2S,4EZ)-1-(tertbutoxycarbonyl)-4-(tert-butoxyimino)-2-pyrrolidinecarboxylic acid | HCID 131725425 | — |
| Product | (2S,4EZ)-4-(tert-butoxyimino)-N-[2-(1H-pyrrol 1-yl)phenyl]-2-pyrrolidinecarboxamide | HCID 131725432 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(tert-butoxyimino)-2-pyrrolidinecarboxylic acid, and 2-(1H-pyrrol-1-yl)phenylamine the title compound was obtained in 83% purity by LC/MS. MS(ESI+): m/z=341.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018988B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-1c852a77c5a54cccaa98b23b69fe92b9 |
| Source note | uspto-grants-2006_03 |