Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1745059Generated: November 3, 2026

Benzo-1,3-dioxole-5-methylamine → HCID 131725440, compound

https://huagongshe.com/reaction/1745059

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzo-1,3-dioxole-5-methylamineHCID 75799—
ReactantPentane, 1-isocyanato-HCID 206036—
ReactantHCID 58714542HCID 58714542—
ProductHCID 131725440HCID 131725440—

Reaction Steps

Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-{[(4-methoxybenzyl)oxy]imino}-2-pyrrolidinecarboxylic acid, 1-isocyanatopentane, and 1,3-benzodioxol-5-ylmethylamine the title compound was obtained in 63% purity by LC/MS. MS(ESI+): m/z=511.4.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07018988B2
Source datasetuspto-grants-2006_03
ORD IDord-33f40cafac4d4df38d4ad7e97273d220
Source noteuspto-grants-2006_03