HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Aminoquinoline → HCID 131725456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Aminoquinoline | HCID 11373 | — |
| Reactant | 3,5-Dichlorophenyl isocyanate | HCID 94460 | — |
| Reactant | (2S,4EZ)-1-(tert-butoxycarbonyl)-4-{[(3,4-dichlorobenzyl)oxy]imino}-2-pyrrolidinecarboxylic acid | HCID 131725417 | — |
| Product | HCID 131725456 | HCID 131725456 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-{[(3,4-dichlorobenzyl)oxy]imino}-2-pyrrolidinecarboxylic acid, 1,3-dichloro-5-isocyanatobenzene, and 6-quinolinamine the title compound was obtained in 66% purity by LC/MS. MS(ESI+): m/z=617.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018988B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-e2eab1c88a2f4b69a40065a536c8d0ee |
| Source note | uspto-grants-2006_03 |