3-Amino-9-ethylcarbazole → HCID 69251329, compound

HRID 1745120Notes

Reaction equation

HRID 1745120 reaction equation
C(OC([N:8]1[CH2:15][C:14](=[CH2:16])[CH2:13][C@H:9]1[C:10]([OH:12])=O)=O)(C)(C)C.[CH2:17]([N:19]1[C:31]2[CH:30]=[CH:29][C:28]([NH2:32])=[CH:27][C:26]=2[C:25]2[C:20]1=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH3:18]>>[CH2:17]([N:19]1[C:31]2[CH:30]=[CH:29][C:28]([NH:32][C:10]([C@@H:9]3[CH2:13][C:14](=[CH2:16])[CH2:15][NH:8]3)=[O:12])=[CH:27][C:26]=2[C:25]2[C:20]1=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH3:18]

Participants

3

Reactant 2

HCID 85883-Amino-9-ethylcarbazoleHCID 21727417(2S)-1-((tert-butoxy)carbonyl)-4-methylidenepyrrolidine-2-carboxylic acid

Product 1

HCID 69251329HCID 69251329, compound

Procedure

Following the general method as outlined in Example 22, starting from 1-(tert-butoxycarbonyl)-4-methyleneproline, and 9-ethyl-9H-carbazol-3-amine the title compound was obtained in 71% purity by LC/MS. MS(ESI+): m/z=320.2.

Sources & evidence

ORD record
ord-5c72326742d84ea9ad047b490e575612
Source dataset
uspto-grants-2006_03
Patent number
US07018988B2

Reaction notes

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