N,N-Diethylethylenediamine → HCID 131725518, compound

HRID 1745170Notes

Reaction equation

HRID 1745170 reaction equation
[CH2:1]([O:4][N:5]=[C:6]1[CH2:10][N:9](C(OC(C)(C)C)=O)[C@H:8]([C:18]([OH:20])=O)[CH2:7]1)[CH:2]=[CH2:3].[CH2:21]([N:23]([CH2:27][CH3:28])[CH2:24][CH2:25][NH2:26])[CH3:22]>>[CH2:1]([O:4][N:5]=[C:6]1[CH2:10][NH:9][C@H:8]([C:18]([NH:26][CH2:25][CH2:24][N:23]([CH2:27][CH3:28])[CH2:21][CH3:22])=[O:20])[CH2:7]1)[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 58714562(2S,4EZ)-4-[(allyloxy)imino)-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acid

Product 1

HCID 131725518HCID 131725518, compound

Procedure

Following the general method as outlined in Example 22, starting from (2S,4EZ)-4-[(allyloxy)-imino]-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acid, and N1,N1-diethyl-1,2-ethanediamine the title compound was obtained in 78% purity by LC/MS. MS(ESI+): m/z=283.0.

Sources & evidence

ORD record
ord-e3c53748f6974bc19e4d8ae8e4a17587
Source dataset
uspto-grants-2006_03
Patent number
US07018988B2

Reaction notes

Loading…