HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridin-3-yl-benzoic acid → HCID 131725595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridin-3-yl-benzoic acid | HCID 1515244 | — |
| Reactant | HCID 12504728 | HCID 12504728 | — |
| Reactant | (2S,4EZ)-1(tert-butoxycarbonyl)-4-(methoxyimino)-2-pyrrolidinecarboxylic acid | HCID 58714586 | — |
| Product | HCID 131725595 | HCID 131725595 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(methoxyimino)-2-pyrrolidinecarboxylic acid, 4-(3-pyridinyl)benzoic acid, and N-(4-{[(2RS)-3-amino-2-hydroxypropyl]oxy}phenyl) acetamide, the title compound was obtained in 66% purity by HPLC. MS(ESI+): m/z=546.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018988B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-41de90f53d71465e84e2c9affd943905 |
| Source note | uspto-grants-2006_03 |