HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorophenylboronic acid → HCID 178498912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorophenylboronic acid | HCID 2733986 | — |
| Reactant | HCID 178498908 | HCID 178498908 | — |
| Product | HCID 178498912 | HCID 178498912 | — |
Reaction Steps
6-(3-Fluoro-phenyl)-4-hydroxy-2-oxo-2H-thiochromene-3-carboxylic acid methyl ester was prepared from 6-bromo-4-hydroxy-2-oxo-2H-thiochromene-3-carboxylic acid methyl ester under conditions analogous to Example 7(a) using 3-fluorophenylboronic acid. 1H NMR (200 MHz, CDCl3): δ (ppm)=8.549 (s, 1H), 7.814-7.664 (m, 2H), 7.463-7.249 (m, 3H), 7.132-7.042 (m, 1H), 4.028 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09149476B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-600d8db61b6c456f94b8488e619b2044 |
| Source note | uspto-grants-2015_10 |