HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyphenylboronic acid → HCID 178498911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyphenylboronic acid | HCID 2733958 | — |
| Reactant | HCID 178498908 | HCID 178498908 | — |
| Product | HCID 178498911 | HCID 178498911 | — |
Reaction Steps
4-Hydroxy-6-(2-methoxy-phenyl)-2-oxo-2H-thiochromene-3-carboxylic acid methyl ester was prepared from 6-bromo-4-hydroxy-2-oxo-2H-thiochromene-3-carboxylic acid methyl ester under conditions analogous to Example 7(a) using 2-methoxy-phenylboronic acid. 1H NMR (200 MHz, CDCl3): δ (ppm)=8.481 (s, 1H), 7.803 (d, 1H), 7.627-7.789 (m, 1H), 7.42-6.92 (m, 4H), 4.022 (s, 3H), 3.82 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09149476B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-6a4759fe6ffa43419456ef7ed6744777 |
| Source note | uspto-grants-2015_10 |