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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1746383Generated: November 3, 2026

Diethyl Ether → HCID 86682254, compound

https://huagongshe.com/reaction/1746383

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl EtherHCID 3283—
ReactantIsobutanolHCID 6560—
ReactantOxalyl chlorideHCID 65578—
ProductHCID 86682254HCID 86682254—

Reaction Steps

Chloro-oxo-acetic acid isobutyl ester was prepared by adding oxalyl chloride (21 μL, 252 μmol) to a solution of isobutanol (21 μL, 226 μmol) in ether (206 μL, 2.0 mmol). The mixture was stirred at room temperature for 15 min and then evaporated.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09150500B2
Source datasetuspto-grants-2015_10
ORD IDord-65eaee9605fc4785a8e647d9e2033d67
Source noteuspto-grants-2015_10