HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86655442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(4-Fluorophenyl)-2-propenoic acid | HCID 98070 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | Methyl tryptophanate hydrochloride | HCID 2734891 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86655442 | HCID 86655442 | 74.7% |
Reaction Steps
The same procedures as in Example 2 were carried out from methyl L-tryptophanate hydrochloride (4.0 g), triethylamine (4.8 mL), 4-fluorocinnamic acid (2.9 g), WSC.HCl (3.3 g), and methylene chloride (150 mL), to give the captioned compound (4.3 g, 74%) as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-8e3236981d894fc099e280eef542311a |
| Source note | uspto-grants-2015_10 |