HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86655462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(2-Fluorophenyl)prop-2-enoic acid | HCID 67977 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | methyl (2R)-2-amino-3-(1H-indol-3-yl)propanoate hydrochloride | HCID 11448200 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86655462 | HCID 86655462 | 86.2% |
Reaction Steps
The same procedures as in Example 2 were carried out from methyl D-tryptophanate hydrochloride (2.5 g), triethylamine (1.6 mL), 2-fluorocinnamic acid (2.0 g), WSC.HCl (2.3 g), and methylene chloride (80 mL), to give the captioned compound (3.1 g, 86%) as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-dce7640cf4a84a27936f1243946a5c67 |
| Source note | uspto-grants-2015_10 |