HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178501464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(2-Fluorophenyl)prop-2-enoic acid | HCID 67977 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | HCID 178501504 | HCID 178501504 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178501464 | HCID 178501464 | 99% |
Reaction Steps
The same procedures as in Example 2 were carried out from methyl Nω-(2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl)-L-argininate hydrochloride (5.0 g), triethylamine (1.8 mL), 2-fluorocinnamic acid (2.1 g), WSC.HCl (2.4 g), and methylene chloride (150 mL), to give the captioned compound (6.1 g, 99%) as an amorphous solid product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-52a4a31faef94181a78591c2ba5ee56b |
| Source note | uspto-grants-2015_10 |