HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Sodium Nalpha-[3-(2-Hydroxyphenyl)acryloyl]-L-Tryptophanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl Nalpha-[3-(2-Acetoxyphenyl)acryloyl]-L-Tryptophanate | HCID 86655437 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Sodium Nalpha-[3-(2-Hydroxyphenyl)acryloyl]-L-Tryptophanate | HCID 86655484 | 94% |
Reaction Steps
The same procedures as in Example 60 were carried out from the compound obtained in Example 2 (5.0 g), 1 mol/L of an aqueous sodium hydroxide solution (37 mL), and methanol (300 mL), to give the captioned compound (4.3 g, 94%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-bff9ee3c94f649798f11c27bb7506fda |
| Source note | uspto-grants-2015_10 |