HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Sodium Nalpha-[3-(4-Hydroxyphenyl)acryloyl]-L-Tryptophanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl Nalpha-[3-(4-Acetoxyphenyl)acryloyl]-L-Tryptophanate | HCID 86655439 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Sodium Nalpha-[3-(4-Hydroxyphenyl)acryloyl]-L-Tryptophanate | HCID 86655486 | 90% |
Reaction Steps
The same procedures as in Example 60 were carried out from the compound obtained in Example 4 (4.5 g), 1 mol/L of an aqueous sodium hydroxide solution (33 mL), and methanol (300 mL), to give the captioned compound (3.7 g, 90%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-fbcf7f8a466b4882baffe9346211a0e9 |
| Source note | uspto-grants-2015_10 |