HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Nalpha-[3-(4-Phenoxyphenyl)acryloyl]-L-Tryptophan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl Nalpha-[3-(4-Phenoxyphenyl)acryloyl]-L-Tryptophanate | HCID 86655450 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Nalpha-[3-(4-Phenoxyphenyl)acryloyl]-L-Tryptophan | HCID 67130594 | 89% |
Reaction Steps
The same procedures as in Example 64 were carried out from the compound obtained in Example 17 (4.9 g), 1 mol/L of an aqueous sodium hydroxide solution (17 mL), and methanol (170 mL), to give the captioned compound (4.2 g, 89%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-eaf6020d534346f8ad39e39fe3a3c10f |
| Source note | uspto-grants-2015_10 |