HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1-Methyl-Nalpha-[3-(4-Phenoxyphenyl)acryloyl]-L-Tryptophan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 1-Methyl-Nalpha-[3-(4-Phenoxyphenyl)acryloyl]-L-Tryptophanate | HCID 86655459 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Methyl-Nalpha-[3-(4-Phenoxyphenyl)acryloyl]-L-Tryptophan | HCID 86655500 | 90% |
Reaction Steps
The same procedures as in Example 64 were carried out from the compound obtained in Example 27 (0.93 g), 1 mol/L of an aqueous sodium hydroxide solution (3.1 mL), and methanol (30 mL), to give the captioned compound (0.81 g, 90%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-5e1289e5bcb7497eaef8add446df180c |
| Source note | uspto-grants-2015_10 |