HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → N-[3-(2-Hydroxyphenyl)acryloyl]-O4-Methyl-L-Tyrosine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl N-[3-(2-Acetoxyphenyl)acryloyl]-O4-Methyl-L-Tyrosinate | HCID 86655464 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-[3-(2-Hydroxyphenyl)acryloyl]-O4-Methyl-L-Tyrosine | HCID 86655503 | 85.4% |
Reaction Steps
The same procedures as in Example 64 were carried out from the compound obtained in Example 35 (6.0 g), 1 mol/L of an aqueous sodium hydroxide solution (38 mL), and methanol (300 mL), to give the captioned compound (4.4 g, 85%) as an amorphous solid product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-371ea22dee7141a4b23d837d75b65bc5 |
| Source note | uspto-grants-2015_10 |