Sodium Hydroxide → HCID 61152778, compound

HRID 1746575Notes

Reaction equation

HRID 1746575 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH:8]=[CH:9][C:10]([NH:12][C@H:13]([C:16]([O:18]C)=[O:17])[CH2:14][OH:15])=[O:11].[OH-].[Na+]>CO>[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH:8]=[CH:9][C:10]([NH:12][C@H:13]([C:16]([OH:18])=[O:17])[CH2:14][OH:15])=[O:11]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 67130619HCID 67130619, compound

Product 1

HCID 61152778HCID 61152778, compoundYield 73%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The same procedures as in Example 64 were carried out from the compound obtained in Example 54 (4.2 g), 1 mol/L of an aqueous sodium hydroxide solution (39 mL), and methanol (390 mL), to give the captioned compound (2.9 g, 73%) as crystals.

Sources & evidence

ORD record
ord-9c870523b32a47b3b897f2f8be27af4f
Source dataset
uspto-grants-2015_10
Patent number
US09150510B2

Reaction notes

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