HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl iodide → HCID 67130666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl iodide | HCID 10962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-tert-Butoxycarbonyl-L-tryptophan | HCID 83169 | — |
| Catalyst | Tetrabutylammonium hydrogen sulfate | HCID 94433 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67130666 | HCID 67130666 | 52% |
Reaction Steps
The same procedures as in Example 137 were carried out from sodium hydroxide (4.6 g), methylene chloride (160 mL), N-tert-butoxycarbonyl-L-tryptophan (10.0 g), 1-iodobutane (19 mL), and tetra-n-butylammonium hydrogensulfate (1.1 g), to give the captioned compound (6.2 g, 52%) as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-d0aa9f4d07684d509dcc56e6bfb59fba |
| Source note | uspto-grants-2015_10 |