HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → N-[3-(3-Methylphenyl)acryloyl]-L-Tryptophan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl N-[3-(3-Methylphenyl)acryloyl]-L-Tryptophanate | HCID 67130739 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-[3-(3-Methylphenyl)acryloyl]-L-Tryptophan | HCID 67130630 | 92% |
Reaction Steps
The same procedures as in Example 149 were carried out from the compound obtained in Example 157 (4.2 g), 1 mol/L of an aqueous sodium hydroxide solution (17 mL), and methanol (170 mL), to give the captioned compound (3.7 g, 92%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-4807ee985622467688747d6c99200afb |
| Source note | uspto-grants-2015_10 |