HRID1746830

反应详情

EQUATION

反应方程式

HRID 1746830 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

The compound obtained in Example 6 was dissolved in water and methanol, to which a catalyst amount of Pd/C was added, and the resultant was stirred for three days in a hydrogen atmosphere. After filtrating the catalyst, the solvent was distilled away, and the resultant was purified using purification step A to obtain the title compound.

WORKUP

后处理

  1. filtrationAfter filtrating the catalyst
  2. distillationthe solvent was distilled away
  3. customthe resultant was purified
  4. custompurification step A