HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-2-hydroxy-4-phenylbutanamide → HCID 89851562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-2-hydroxy-4-phenylbutanamide | HCID 13882355 | — |
| Reactant | HCID 89851665 | HCID 89851665 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 89851562 | HCID 89851562 | 129.9% |
Reaction Steps
Coupling of sodium 2-(5-benzyl-4,5,6,7-tetrahydro-2H-pyrazolo[4,3-c]pyridin-2-yl)nicotinate (106 mg, 0.297 mmol) and 3-amino-2-hydroxy-4-phenylbutanamide (80 mg, 0.412 mmol) in N,N-dimethylformamide (10 mL) according to example 1.3 and work-up gave 197 mg of the title compound a amorphous solid; ESI-MS [M+H]+: 511.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150545B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-91127d9656634e6eb42f11f8c9f8f987 |
| Source note | uspto-grants-2015_10 |