HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | 1-(6-(Hydroxymethyl)pyridin-2-yl)ethanone | HCID 10329447 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-[6-(Hydroxymethyl)pyridin-2-yl]ethanone oxime | HCID 136346367 | — |
Reaction Steps
To a solution of 1643 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone in 25 ml of ethanol was added 0.72 ml of a 50% aqueous hydroxylamine solution, followed by stirring overnight. The reaction solution was concentrated under reduced pressure to obtain 1806 mg of 1-[6-(hydroxymethyl)pyridin-2-yl]ethanone oxime as an amorphous substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150541B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-cbce93e8394845eaade63b03730db94c |
| Source note | uspto-grants-2015_10 |