1,4-Dichlorobenzene → HCID 89586238, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of [(1-phenyl-1H-pyrazol-5-yl)amino]acetonitrile (1.20 g) in dichlorobenzene (15.0 mL) was added oxalyl chloride (0.922 g) at room temperature, and the mixture was stirred at 100° C. for 12 hr. The reaction mixture was purified by silica gel column chromatography (dichloromethane/methanol) to give the title compound (0.850 g).

Provenance & Evidence