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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1748064Generated: October 31, 2026

HCID 66748164, compound → HCID 66823919, compound

https://huagongshe.com/reaction/1748064

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66748164HCID 66748164—
CatalystAdams' catalystHCID 345198—
SolventMethanolHCID 887—
ProductHCID 66823919HCID 6682391937.5%

Reaction Steps

A mixture of 9-(4-propoxyphenyl)-3,4-dihydropyrido[2,1-c][1,2,4]thiadiazine 2,2-dioxide (300 mg) and platinum(IV) oxide (32.1 mg) in MeOH (10 mL) was stirred at room temperature under H2 for 20 hr. The reaction mixture was filtered by Celite and the filtrate was concentrated in vacuo. The residue was recrystallized from EtOAc-MeOH to give the title compound (114 mg) as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09150591B2
Source datasetuspto-grants-2015_10
ORD IDord-9a6a7a761e8542df8abdba180699ade5
Source noteuspto-grants-2015_10