HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobenzene → 1,4-Di-2-butylhexylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobenzene | HCID 7804 | — |
| Reactant | 2-Butylhexylbromide | HCID 15752615 | — |
| Reactant | 1,4-Di-2-ethylhexylbenzene | HCID 86719906 | — |
| Product | 1,4-Di-2-butylhexylbenzene | HCID 86719905 | — |
Reaction Steps
1,4-Di-2-butylhexylbenzene (20b) was synthesized according to the same procedure as 20a with 1,4-dibromobenzene (24 g, 0.102 mol) and 2-butylhexylbromide (54.1 g, 0.245 mol). (18.3 g, 50%) 1H NMR (CDCl3): δ 0.84-0.92 (12H, m), 1.23-1.34 (24H, m), 1.54-1.65 (2H, m), 2.49 (4H, d), 7.03 (4H, S). MS (EI): calcd, 358.6. found M+, 358.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09153785B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-79d747c2a5fb4bebbfa5ad1377175449 |
| Source note | uspto-grants-2015_10 |