2-Aminothiophenol → HCID 136043207, compound

HRID 1748970Notes

Reaction equation

HRID 1748970 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[SH:8].[Br:9][C:10]1[CH:11]=[C:12]([CH:15]=[CH:16][C:17]=1[OH:18])[CH:13]=O>CO>[S:8]1[C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[N:1]=[C:13]1[C:12]1[CH:15]=[CH:16][C:17]([OH:18])=[C:10]([Br:9])[CH:11]=1

Participants

4

Reactant 2

HCID 87132-AminothiophenolHCID 763083-Bromo-4-hydroxybenzaldehyde

Product 1

HCID 136043207HCID 136043207, compoundYield 38%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a methanol solvent, a solution including 2-aminothiophenol (1.0 eq.) and 3-bromo-4-hydroxybenzaldehyde (1.0 eq.) was stirred at room temperature. The produced precipitate was filtered and the filtered product was washed with cold methanol to obtain Compound 26.

Workup

  1. filtrationThe produced precipitate was filtered
  2. washthe filtered product was washed with cold methanol

Sources & evidence

ORD record
ord-75d928661ed241dfb82c1ab2605a5310
Source dataset
uspto-grants-2015_10
Patent number
US09155690B2

Reaction notes

Loading…