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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1749870Generated: November 2, 2026

HCID 178520024, compound → HCID 178520023, compound

https://huagongshe.com/reaction/1749870

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178520024HCID 178520024—
CatalystHCID 178418406HCID 178418406—
SolventEthyl AcetateHCID 8857—
ProductHCID 178520023HCID 17852002367.4%

Reaction Steps

A solution of (5-bromo-1H-indazol-3-yl)-methanol (0.267 g, 1.18 mmol) in ethyl acetate (12 mL) was added with manganese dioxide (1.03 g, 11.8 mmol), and the mixture was stirred overnight at room temperature. The reaction mixture was filtered through Celite, and then the filtrate was concentrated to obtain 5-bromo-1H-indazole-3-carbaldehyde (0.179 g, 67%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09156827B2
Source datasetuspto-grants-2015_10
ORD IDord-3426e0f2beb3432bab438b67c4e47f35
Source noteuspto-grants-2015_10