Hydrochloric Acid → HCID 67144985, compound

Participants

Reaction Steps

To a solution of Example 8B (1.6 g, 6.38 mmol) in ether (20 mL) was added LiAlH4 (1.2 g, 32 mmol). The mixture was stirred at room temperature for four hours. The mixture was acidified carefully with 5% HCl and extracted with ethyl acetate (100 mL×3) and washed with water, brine and dried over Na2SO4. After evaporation, the crude product was loaded on a column and eluted with 10% ethyl acetate in hexane to give title compound.

Provenance & Evidence