HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1,1'-Biphenyl)-4-methanol → [1,1′-Biphenyl]-4-ylmethyl 2-propenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1,1'-Biphenyl)-4-methanol | HCID 19186 | — |
| Reactant | (1,1'-Biphenyl)-2-methanol | HCID 76229 | — |
| Product | [1,1′-Biphenyl]-4-ylmethyl 2-propenoate | HCID 15621059 | — |
Reaction Steps
The same process as in Synthetic Example 1 was conducted except that the ortho-phenylbenzyl alcohol in Synthetic Example 1 was changed to para-phenylbenzyl alcohol. Consequently, 22.4 g of para-phenylbenzyl acrylate was obtained. The obtained para-phenylbenzyl acrylate was solid at ordinary temperature and had a melting point of 32° C. and a refractive index of 1.5920 at 40° C. The measurement result of 1H-NMR is shown below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09156931B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-849c6c950ff8421aaa766f5f38443c0d |
| Source note | uspto-grants-2015_10 |