HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 59610468, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59611113 | HCID 59611113 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59610468 | HCID 59610468 | — |
Reaction Steps
6,6′-bis-bromomethyl-2,4,2′,4′-tetramethoxy-biphenyl (685 mg) was dissolved in DCM (3.0 mL), and 1M BBr3 in DCM (16.4 mL) was slowly added. After stirring for 2 days, the mixture was poured on to ice and concentrated. The crude material was used for the next step without a further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09156823B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-c11b70551c984a11a63c256b530aecf6 |
| Source note | uspto-grants-2015_10 |