HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methoxycarbonyl-2-phenylglycine → HCID 69676609, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methoxycarbonyl-2-phenylglycine | HCID 596264 | — |
| Reactant | [1-(2-{5-[6-(4-{2-[1-(2-tert-Butoxycarbonylamino-2-phenyl-acetyl)-pyrrolidin-2-yl]-3H-imidazol-4-yl}-phenyl)-naphthalen-2-yl]-1H-imidazol-2-yl}-pyrrolidine-1-carbonyl)-2-methyl-propyl]-carbamic acid methyl ester | HCID 69675475 | — |
| Product | HCID 69676609 | HCID 69676609 | 46.6% |
Reaction Steps
This compound was synthesized using the procedure used to synthesize [1-(2-{5-[6-(4-{2-[1-(2-tert-Butoxycarbonylamino-2-phenyl-acetyl)-pyrrolidin-2-yl]-3H-imidazol-4-yl}-phenyl)-naphthalen-2-yl]-1H-imidazol-2-yl}-pyrrolidine-1-carbonyl)-2-methyl-propyl]-carbamic acid methyl ester using Methoxycarbonylamino-phenyl-acetic acid (0.079 g, 0.380 mmol) giving the title compound (0.100 g, 46.6% yield) as a white solid. LCMS-ESI+: calc'd for C49H52N8O6: 848.40 (M+); Found: 849.50 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09156823B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-ba568bd962f74aac82da8a7db1ea1b10 |
| Source note | uspto-grants-2015_10 |