N-Methoxycarbonyl-2-phenylglycine → HCID 69676609, compound

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Reaction Steps

This compound was synthesized using the procedure used to make [1-(2-{5-[6-(4-{2-[1-(2-tert-Butoxycarbonylamino-2-phenyl-acetyl)-pyrrolidin-2-yl]-3H-imidazol-4-yl}-phenyl)-naphthalen-2-yl]-1H-imidazol-2-yl}-pyrrolidine-1-carbonyl)-2-methyl-propyl]-carbamic acid methyl ester using Methoxycarbonylamino-phenyl-acetic acid (0.047 g, 0.224 mmol) to give [1-(2-{5-[6-(4-{2-[2-(2-Methoxycarbonylamino-2-phenyl-acetyl)-2-aza-bicyclo[2.2.1]hept-3-yl]-3H-imidazol-4-yl}-phenyl)-naphthalen-2-yl]-1H-imidazol-2-yl}-pyrrolidine-1-carbonyl)-2-methyl-propyl]-carbamic acid methyl ester (0.044 g, 34.8% yield). LCMS-ESI+: calc'd for C49H52N8O6: 848.40 (M+); Found: 849.96 (M+H+).

Provenance & Evidence