HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 58080360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 58080352 | HCID 58080352 | — |
| Product | HCID 58080360 | HCID 58080360 | — |
Reaction Steps
50 mg tert-butyl 4-[4-(4,5-dihydrooxazol-2-yl)-phenoxy]-piperidine-1-carboxylate are taken and mixed with 6 ml of a (5/1) dichloromethane/trifluoroacetic acid mixture. The reaction mixture is stirred at ambient temperature and after 15 min it is cautiously mixed with a saturated NaHCO3 solution. The organic phase is dried and evaporated to dryness. 20 mg (V-2) are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09161927B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-2aa3b7e8285042b7a975f53164003c69 |
| Source note | uspto-grants-2015_10 |