HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → Diethyl phenylmalonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | Iodobenzene | HCID 11575 | — |
| Product | Diethyl phenylmalonate | HCID 66514 | 90% |
Reaction Steps
Following General Procedure A (90° C., 30 hours), diethyl malonate (240 mg, 1.5 mmol) is coupled with iodobenzene (112 μL, 1.0 mmol) to give 90% diethylphenylmalonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162953B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-aabcfb486f514f7e83f6e3575901ae9e |
| Source note | uspto-grants-2015_10 |