HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethylphenol → Phenyl 3,5-xylyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethylphenol | HCID 7948 | — |
| Reactant | Chlorobenzene | HCID 7964 | — |
| Product | Phenyl 3,5-xylyl ether | HCID 117541 | 60% |
Reaction Steps
Following General Procedure C (140° C., 30 hours), 3,5-dimethyl-phenol (183 mg, 1.5 mmol) is coupled with chlorobenzene (102 μL, 1.0 mmol) to give 60% 1,3-dimethyl-5-phenoxybenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162953B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-6aac12387ae24f668e55bd7bdd469401 |
| Source note | uspto-grants-2015_10 |