Phosphoric Acid → HCID 86673897, compound

HRID 1752160Notes

Reaction equation

HRID 1752160 reaction equation
[CH2:1]([NH:4][C:5]1[N:10]=[C:9]([NH:11][CH2:12][CH2:13][CH3:14])[N:8]=[C:7]([N:15]([CH3:18])[O:16][CH3:17])[N:6]=1)[CH2:2][CH3:3].[P:19](=[O:23])([OH:22])([OH:21])[OH:20]>C(#N)C>[P:19](=[O:20])([OH:23])([OH:22])[OH:21].[CH2:1]([NH:4][C:5]1[N:10]=[C:9]([NH:11][CH2:12][CH2:13][CH3:14])[N:8]=[C:7]([N:15]([CH3:18])[O:16][CH3:17])[N:6]=1)[CH2:2][CH3:3]

Participants

4

Reactant 2

HCID 1004Phosphoric AcidHCID 57340959N-(4,6-Bis(propylamino)-1,3,5-triazin-2-yl)-N,O-dimethylhydroxylamine

Product 1

HCID 86673897HCID 86673897, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

To (XXXV) in acetonitrile at ambient temperature were added two molar equivalents of phosphoric acid. The mixture was stirred for 2 days, then the solid that was formed was collected by filtration and dried on the filter under a nitrogen stream (Phosphoric Acid Salt Form A; FIG. 27).

Workup

  1. customthe solid that was formed
  2. filtrationwas collected by filtration
  3. customdried on the
  4. filtrationfilter under a nitrogen stream (Phosphoric Acid Salt Form A; FIG. 27)

Sources & evidence

ORD record
ord-f082b065c2164ec6a8441bd7b871db69
Source dataset
uspto-grants-2015_10
Patent number
US09162992B2

Reaction notes

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