Water → HCID 71254034, compound

Participants

Reaction Conditions

Reaction Steps

9-(3-azido-2-fluoropropyl)-3,6-dibromo-9H-carbazole (60 mg, 0.14 mmol) and triphenylphosphine (44 mg, 0.168 mmol) were combined in 0.5 mL of THF and stirred overnight at 60° C. Upon completion 1 ml of H2O was added and the mixture was stirred for 1 hour. The mixture was extracted with EtOAc. The organic layer was washed with H2O, brine, and dried over Na2SO4 and concentrated to a white foam. This xmaterial was used in the next step without further purification.

Provenance & Evidence