HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Chlorophenoxy)ethanol → 5,7-Diethyl-2-[-2-(4-chlorophenoxy)ethoxy]-[1,2,4]triazolo[1,5-a]pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Chlorophenoxy)ethanol | HCID 15907 | — |
| Reactant | 2-Methanesulfonyl-5,7-diethyl-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 86719320 | — |
| Product | 5,7-Diethyl-2-[-2-(4-chlorophenoxy)ethoxy]-[1,2,4]triazolo[1,5-a]pyrimidine | HCID 76684794 | 80% |
Reaction Steps
The title compound was prepared according to the experimentals described for Example 14 above from 2-methanesulfonyl-5,7-diethyl-[1,2,4]triazolo[1,5-a]pyrimidine and 2-(4-chlorophenoxy)ethan-1-ol in 80% yield. EM (calc.): 346.1; MS (ESI) m/e: 347.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163027B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-1a9be86d3f074314be306d62ca54be26 |
| Source note | uspto-grants-2015_10 |