Hexafluoroacetylacetone → HCID 90149787, compound

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Reaction Steps

The title compound was prepared according to the experimentals described for Example 23 above from 3-{[2-(4-chlorophenoxy)ethyl]sulfanyl}-1H-1,2,4-triazol-5-amine and hexafluoroacetylacetone in 32% yield; EM (calc.): 442.0; MS (ESI) m/e: 443.0 (M+H)+. 1H NMR (DMSO-d6, 400 MHz) δ ppm: 8.40 (s, 1H), 7.32 (d, 2H), 7.01 (d, 2H), 4.36 (t, 2H), 3.71 (t, 2H). 19F NMR (DMSO-d6, 376 MHz) δ ppm: −66.84 (s), −67.45 (s).

Provenance & Evidence