HCID 15752645, compound → HCID 86719332, compound

HRID 1752824Notes

Reaction equation

HRID 1752824 reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]2[N:9]=[C:10]([SH:12])[N:11]=[C:4]2[N:3]=1.Br[CH2:14][CH2:15][O:16][CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1>>[CH:17]1([O:16][CH2:15][CH2:14][S:12][C:10]2[N:11]=[C:4]3[N:3]=[C:2]([CH3:1])[CH:7]=[C:6]([CH3:8])[N:5]3[N:9]=2)[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1

Participants

3

Reactant 2

HCID 15752645HCID 15752645, compoundHCID 178426287HCID 178426287, compound

Product 1

HCID 86719332HCID 86719332, compoundYield 78%

Procedure

The title compound was prepared according to the experimentals described for Example 1 above from 5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidine-2-thiol and 2-bromoethoxy cyclohexane in 78% yield; EM (calc.): 306.2; MS (ESI) m/e: 307.2 (M+H)+.

Sources & evidence

ORD record
ord-0b5e52529e994432bea8a27fd02ff16c
Source dataset
uspto-grants-2015_10
Patent number
US09163027B2

Reaction notes

Loading…