2-(p-Chlorophenylthio)ethanol → 2-{2-[(4-Chlorophenyl)sulfanyl]ethoxy}-5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidine

Participants

Reaction Steps

The title compound was prepared according to the experimentals described for Example 11 above from 2-methanesulfonyl-5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidine and 2-[(4-chlorophenyl)sulfanyl]ethan-1-ol in 38% yield. 1H NMR (DMSO-d6, 400 MHz) δ ppm: 7.47 (dd, 1H), 7.45 (dd, 1H), 7.39 (dd, 1H), 7.37 (dd, 1H), 7.08 (s, 1H), 4.51 (t, 2H), 3.45 (t, 2H), 2.62 (s, 3H), 2.52 (s, 3H).

Provenance & Evidence