HuagongsheHuagongshe Chemistry Print Report · For research reference only
Linoleic Acid → Oleyl linoleate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Linoleic Acid | HCID 5280450 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Oleyl linoleate | HCID 6436476 | — |
Reaction Steps
Oleyl linoleate was prepared by refluxing linoleic acid (1 g) and Oeyl alcohol (1 ml) in CH2Cl2 (20 ml) and concentrated H2SO4 (10 μl) overnight. The product was slightly pink and was purified by flash chromatography. The resultant Oeyl linoleate was subjected to the Simmons-Smith procedure described above to generate DCPLA-oleyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09163032B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-833bb285c7dd495e9b93d9aad39f8e43 |
| Source note | uspto-grants-2015_10 |