Sulfuric Acid → 604-33-1

Participants

Reaction Steps

DCPLA (1 g), cholesterol (1 g), CH2Cl2 (20 ml), and concentrated H2SO4 (1 μl) were combined and refluxed overnight. The product was washed with sodium phosphate (pH 7.0, 5 ml) and purified by flash chromatography to yield the DCPLA-cholesteryl ester. Linoleic acid (1 g), cholesterol (1 g), CH2Cl2 (20 ml), and concentrated H2SO4 (20 μl) were combined and refluxed overnight. The product was washed with sodium phosphate (pH 7.0, 5 ml) and purified by flash chromatography to yield the cholesteryl linoleate.

Provenance & Evidence