HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → Methyl 2-(3-bromo-5-formyl-4-hydroxyphenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Methyl 2-(3-formyl-4-hydroxyphenyl)acetate | HCID 12374099 | — |
| Product | Methyl 2-(3-bromo-5-formyl-4-hydroxyphenyl)acetate | HCID 57198039 | 80.1% |
Reaction Steps
Proceeding as in Reference 9, but substituting methyl 3-formyl-4-hydroxy-phenyl-acetate (50 g, 0.258 mol) and N-bromosuccinimide (45.92 g, 0.258 mole), gave methyl 3-bromo-5-formyl-4-hydroxyphenylacetate (56.4 g, 80%) as a yellow amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162986B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-ea86f2ad208546f3bf8adb1011aa806a |
| Source note | uspto-grants-2015_10 |