HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66986016, compound → HCID 86628074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66986016 | HCID 66986016 | — |
| Reactant | HCID 86628075 | HCID 86628075 | — |
| Product | HCID 86628074 | HCID 86628074 | 54.9% |
Reaction Steps
Proceeding as in Reference 19, but substituting 1-[3-bromo-4-(2-ethoxyethoxymethoxy)benzyl]-3-tert-butylurea (1.0 g, 2.9 mmol) and 5-fluoro-2-(2-methoxy-ethoxymethoxy)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzaldehyde (29 mL, 0.1 mM in toluene, 2.9 mmol) gave 1-tert-butyl-3-[5′-fluoro-3′-formyl-6,2′-bis-(2-methoxyethoxymethoxy)biphenyl-3-ylmethyl]-urea (0.854 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162986B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-14ecb6069db948559b4d2da2f9f7f111 |
| Source note | uspto-grants-2015_10 |