Benzenepropanoyl chloride → HCID 86628078, compound

HRID 1752920Notes

Reaction equation

[CH:1]([C:3]1[CH:4]=[C:5]([S:17]([NH2:20])(=[O:19])=[O:18])[CH:6]=[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:8]=1[O:9][CH3:10])=[O:2].[C:21]1([CH2:27][CH2:28][C:29](Cl)=[O:30])[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[CH:1]([C:3]1[CH:4]=[C:5]([S:17]([NH:20][C:29](=[O:30])[CH2:28][CH2:27][C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)(=[O:19])=[O:18])[CH:6]=[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:8]=1[O:9][CH3:10])=[O:2]

Participants

Reactant 2

HCID 64801Benzenepropanoyl chloride

HCID 86607715HCID 86607715, compound

Product 1

HCID 86628078HCID 86628078, compound

Procedure

Proceeding as in Reference 21, but substituting 5-formyl-6-methoxy-biphenyl-3-sulfonamide and 3-phenyl-propanoyl chloride, gave 5-formyl-6-methoxy-N-(3-phenyl-propanoyl)-biphenyl-3-sulfonamide.

Sources & evidence

ORD record: ord-b7f97545eae74ce5833e59f01e95e439
Source dataset: uspto-grants-2015_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09162986B2

Reaction notes

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